Diethanolisopropanolamine (DEIPA)


DEIPA
EC / List no.: 229-764-5
CAS no.: 6712-98-7
Mol. formula: C7H17NO3


1-(N,N-bis(2-hydroxyethyl)amino)propan-2-ol
1-(N,N-Bis(2-hydroxyethyl)amino)propan-2-ol
1-(N,N-bis(2-Hydroxyethyl)amino)propan-2-ol
1-(N,N-bis(2-hydroxyethyl)amino)propan-2-ol
2-Propanol, 1-[bis(2-hydroxyethyl)amino]-
2-propanol, 1-[bis(2-hydroxyethyl)amino]-
N,N-Bis(2-hydroxyethyl)-2-pro panolamine
N,N-Bis(2-hydroxyethyl)-2-propanolamine

2-Propanol, 1-[bis(2-hydroxyethyl)amino]-

1-(N,N-Bis(2-hydroxyethyl)amino)propan-2-ol
1-(N,N-bis(2-hydroxyethyl)amino)propan-2-ol
1-(N,N-bis(2-hydroxyethyl)amino)propan-2-ol
1-[Bis(2-hydroxyethyl)amino]-2-propanol
1-[bis(2-hydroxyethyl)amino]propan-2-ol
DEIPA
Diethanolisopropanolamin
Diethanolisopropanolamine (DEIPA)

Applications: Grinding Aid in Cement and concrete.


Diethanol lsopropanolamine  is an alkanol amine used in formulation of concrete admixtures and cement additives that requires high early and final strengths.

Use
DEIPA is used in the following conditions and applications.

• For increasing the final and early strength of concrete.
• Precast concrete industry.
• For concrete admixture formulations where early strength is desired,
• Concreting work requiring high early and ultimate strenght.

Application Details
It is generaly compatible to use DEIPA in concrete admixture recipes with Naphthalene Sulfonate, Melamine Sulfonate, Lignin Sulfonate and Polycarboxylate based raw materials.


Diethanol lsopropanolamine (DEIPA) is an alkanol amine used in formulation of concrete admixtures and cement additives. 
Moreover being a good grinding aid in the cement mill, DEIPA raises the potency of cement at all hydration ages, and cements blended with slag and fly ash tends to show bigger response to the chemical. 
Diethanol Isopropanolamine (DEIPA) is frequently used in cement grinding aids to restore Triisopropanolamine and Triethanolamine in grinding aid raw materials. 
DEIPA is a new green grinding aid raw material.

Market Dynamics
As DEIPA helps in strengthen the cement grade at all stages, producers of cement grinding aid now prefer DEIPA as a substitute for TIPA & TEA to save cost and get better quality products. 
DEIPA has recently acquired strong foothold in different applications areas such as cement grinding aid, surfactant and others.
Globally, the market for DEIPA is mainly driven by growing demand for cement grinding aid. 
Cement grinding aid application accounted for over 70% of total downstream consumption of diethanol isopropanolamine (DEIPA) in global. 
On the other hand, DEIPA prevent cement particles from re-agglomeration, or re-adhering, during and after the grinding process and make it possible to streamline the cement-making process by increasing process efficiency and material fluidity. 
The use of DEIPA in cement grinding aid applications also assists in lowering the energy costs of industrial mills which creates lucrative opportunities for DEIPA market in near future.
Content 85% segment was the largest with around 60% market share of the overall market in 2017. 
The content 85% grade is used in cement production due to its benefitting physical properties such as a clear, viscous, pale yellow liquid, or colorless chemical which offers freezing point of 21°C, boiling point (0.6mmHg) 145? (lit.), and can be dissolved into many organic solvents and water. 
Growing urbanization and rising construction activities create demand for good quality raw material such as cement which directly creates a positive impact on DEIPA market and is required to encourage the utilization of diethanol isopropanolamine over the foreseeing time span. 
In light of regional analysis, China was accountable for a huge portion of global market share in 2017, and held around 35% of the total market. 
The region is boosted by elevated demand from construction activities in various segments such as commercial, residential, and infrastructure area that generated a notable growth of diethanol isopropanolamine market demand constantly.

RESEARCH ON PROPERTIES AND THE HYDRATION OF PORTLAND LIMESTONE CEMENT WITH DIETHANOL-ISOPROPANOLAMINE 
XIAOLEI LU*, **, SHUXIAN WANG*, CHUANHAI LI*, **, # ZHENGMAO YE*, **, # XIN CHENG*, ** *
School of Materials Science and Engineering, University of Jinan, Jinan, Shandong 250022, China 
**Shandong Provincial Key Laboratory of Preparation and Measurement of Building Materials, Jinan, Shandong 250022, 
China # E-mail: mse_yezm@163.com (Zhengmao Ye), mse_chengxin@163.com (Xin Cheng) Submitted December 19, 2017;
 accepted March 27, 2018 
Keywords: Diethanol-isopropanolamine, Portland limestone cement, Properties, Hydration mechanism 


Diethanol-isopropanolamine (DEIPA) is a new type of alkanolamine used as grinding aids for Portland cement. 
In this study, the effect of DEIPA on properties of Portland limestone cement (PLC) were investigated by measuring strength of mortar, setting time, compatibility of cement and superplasticizers. 
A combination of isothermal calorimetry, scanning electron microscopy and mercury intrusion porosimetry was used to investigate the hydration kinetics. 
The results indicate that the addition of DEIPA markedly enhances the early and late strength of mortar, which gains a 4.4 MPa increment (28.7 %) at 3 d and a 6.3 MPa increment (20.3 %) at 28 d, respectively, and is not significant differences in the setting time. 
However, the compatibility of cement and superplasticizer becomes poor in the cement paste containing DEIPA. 
The working mechanism of DEIPA accelerates the hydration of aluminate and alite, and promotes the formation of AFt and monocarboaluminate, as well as the transformation of AFt to AFm. 
Besides, the addition of DEIPA results in uniformly overlaps hydration products and improves microstructure in hardened cement pastes

Diethanol-isopropanolamine (DEIPA) is a new alkanolamine in cement grinding agents. 
Figure 1 shows a schematic representation of the chemical structure of DEIPA. 
There have been a few studies on the influence of DEIPA on the hydration of Portland cement. 
L. Jardine [17] investigated that DEIPA was preferred for improving early strength when admixed into cementitious compositions. 
Riding [18] observed that DEIPA increased the early age mortar strength and affected the morphology of calcium hydroxide 
(CH). Ma [19, 20] also observed that DEIPA can increase the early and late strength and promote the formation of AFt and microcrystalline CH at early stages. 
J. Cheung [21] reported DEIPA can enhance the compressive strength of the limestone blended cement. 
Nevertheless, the effect of DEIPA on the properties and hydration process of PLC is unknown. 
In this work, DEIPA was added into PLC to investigate the effect on properties (compressive strength, setting time and compatibility of cement and superplasticizer) and hydration kinetics. 
In addition, the mechanism of cement hydration in the presence of DEIPA was discussed


Diethanol Isopropanolamine (DEIPA) is often used in cement grinding aids to replace Triethanolamine and Triisopropanolamine in grinding aid raw materials. 
Diethanol Isopropanolamine is a new green grinding aids raw materials.


The method of Joint Production isopropanolamine
Abstract
The invention belongs to chemical building material field, the method relating to Joint Production DEIPA and TIPA.
The present invention has industrialized production environmental protection, production efficiency height, better economic benefit, facilitates the features such as grinding aid formula adjustment.
Step is as follows: A, in reactor 1, is continuously added to PO in ammonia spirit, controls reaction temperature and pressure, and reaction is to obtaining intermediate products;B, step A gained intermediate products being gone to vacuum rectification tower, tower top distillates ammoniacal liquor recovered liquid, and side line distillates MIPA, collect at the bottom of tower for high boiling substance;C, step B gained MIPA being added reactor 2, be continuously added to EO, control reaction temperature and pressure, reaction is to obtaining DEIPA;High boiling substance at the bottom of step B gained tower being added reactor 3, is continuously added to PO, control reaction temperature and pressure, reaction is to obtaining TIPA.


The invention belongs to chemical building material field, the method relating to producing isopropanolamine, it is specifically related to Joint Production diethanol list isopropyl Hydramine (vehicle economy IPA) and the method for triisopropanolamine (being called for short TIPA), DEIPA and TIPA can be used as cement grinding aid.

Background technology
Grinding aid is the additive in cement pulverizing course, it is possible to increase mill efficiency.
DEIPA and TIPA is that cement helps The main component of grinding agent, adds DEIPA and TIPA and can improve cement grinding efficiency largely, simultaneously in grinding aid DEIPA can increase substantially cement early stage and later strength, and TIPA can increase substantially the later strength of cement.


Major Applications are as follows:

● Cement Grinding Aid
● Surfactant
● Others


Diethanol Isopropanolamine (DEIPA) is often used in cement grinding aids to replace Triethanolamine and Triisopropanolamine in grinding aid raw materials. 
Diethanol Isopropanolamine is a new green grinding aids raw materials.


Description
Diethanol-isopropanolamine (DEIPA) is an alkanol amine used in the formulation of cement additives and concrete admixtures. 
Besides being a good grinding aid in the cement mill, DEIPA increases the strength of cements at all hydration ages, and cements blended with fly ash and slag tend to show a greater response to the chemical.In this research, the impact of DEIPA on the hydration of blast furnace slag blended cements is studied using several analytical techniques, such as quantitative X-ray diffraction with Rietveld refinement (QXRD), scanning electron microscopy (SEM) with backscattered electron image analysis, thermogravimetric analysis (TGA), and chemical shrinkage. 
Isothermal calorimetry was also used to demonstrate the impact of DEIPA on the reactivity of slag in blended cements.
Compressive strength tests were performed to assess the impact of the amine in such cements.
It is demonstrated that DEIPA increases the mortar strength by enhancing primarily the aluminate hydration and the morphology and composition of the hydrates, such as calcium hydroxide and C-S-H.The visual observation was confirmed by isothermal calorimetry, where DEIPA was found to directly enhance the rate of reaction of granulated blast-furnace slag after 48 hours of hydration


    
DEIPA improves both initial strength and later strength of cement. 
DEIPA also heps to get better effect of later strength than TIPA does.

Diethanol-isopropanolamine (DEIPA) is a tertiary alkanolamine used in the formulation of cement grinding-aid additives and concrete early-strength agents.

Description
Diethanol-isopropanolamine (DEIPA) is an alkanol amine used in the formulation of cement additives and concrete admixtures. 
Besides being a good grinding aid in the cement mill, DEIPA increases the strength of cements at all hydration ages, and cements blended with fly ash and slag tend to show a greater response to the chemical

Diethanolisopropanolamine (DEIPA)
Diethanolisopropanolamine (DEIPA) is an alkanol amine used in the formulation of cement additives and concrete admixtures. 
Besides being a good grinding aid in the cement mill, DEIPA increases the strength of cements at all hydration ages, and cements blended with fly ash and slag tend to show a greater response to the chemical.

A grinding aid (DEIPA) is a specialty chemical agent used to make it easier to grind and mix cement. 
Specifically, grinding aids prevent cement particles from re-agglomeration, or re-adhering, during and after the grinding process. 
Grinding aids make it possible to streamline the cement-making process by increasing process efficiency and material fluidity. 
These benefits of cement grinding aid use also contribute to lower energy costs on the part of industrial mills.


The grinding aid began to gain popularity in the mid-20th century as a reliable tool for cement processing. 
Its effectiveness and reputation for reliability lie in its ability to reduce surface tension between cement particles brought on by the stress of the grinding process. 
Chemical compounds known for their polar properties, such as alkanolomines, disperse charges on the surface of the cement particle. 
This covering of charges prevents individual particles from clumping together.
Hydration is also an important factor in the grind aid process. 
When a grinding aid (DEIPA) comes in contact with a cement particle, it forms an instant gel around the particle. 
This gel hydrates the grain and initially serves as a barrier from other cement particles. With time, the gel crystallizes. 
This crystallization allows the cement particle to attach itself to others, forming a fluid lattice structure.

DEIPA advantages compared with TIPA:

According to the research, their effects on cement properties is better than the ordinary cement grinding aids as TEA & TIPA, the cement compressive strength in all ages were improved when DEIPA was added to cements. 
The effect of DEIPA and TIPA were similar on cement properties including normal consistency, setting time, fineness and fluidity, etc. 
DEIPA is excellent cement grinding aid.

The method of Joint Production isopropanolamine
Abstract
The invention belongs to chemical building material field, the method relating to Joint Production DEIPA and TIPA.
The present invention has industrialized production environmental protection, production efficiency height, better economic benefit, facilitates the features such as grinding aid formula adjustment.
Step is as follows: A, in reactor 1, is continuously added to PO in ammonia spirit, controls reaction temperature and pressure, and reaction is to obtaining intermediate products;B, step A gained intermediate products being gone to vacuum rectification tower, tower top distillates ammoniacal liquor recovered liquid, and side line distillates MIPA, collect at the bottom of tower for high boiling substance;
C, step B gained MIPA being added reactor 2, be continuously added to EO, control reaction temperature and pressure, reaction is to obtaining DEIPA;
High boiling substance at the bottom of step B gained tower being added reactor 3, is continuously added to PO, control reaction temperature and pressure, reaction is to obtaining TIPA.

With Diethanolisopropanolamine as the core material made of grinding aid in improving their strength of cement for three days at the same time, can improve the strength of 28 days.

Diethanol Isopropanolamine (DEIPA) appearance mild yellow or colorless, Very light ammonia odor with flash point minimum 112°C, and density 1.083 g/cm3 (20°C).

Molecular Formula: C7H17NO3

Usage:
Diethanol Isopropanolamine (DEIPA) is an alkanol amine. 
Mainly used in the formulation of cement additives and concrete admixtures. 
Diethanol Isopropanolamine (DEIPA used to replace Triethanolamine (TEA) and Triisopropanolamine, significantly increase the early and late strength of mortar or cement. 
Diethanol Isopropanolamine (DEIPA) also improves microstructure in hardened cement paste.


CEMENT GRINDING AID : DEIPA
Diethanolisopropanolamine
Besides being a good grinding aid in the cement mill, DEIPA increases the strength of cements at all hydration ages, and cements blended with fly ash and slag tend to show a greater response to the chemical.
In this research, the impact of DEIPA on the hydration of blast furnace slag blended cements is studied using several analytical techniques, such as quantitative X-ray diffraction with Rietveld
Cement Grinding Aids 
Deipa With Best Price 
DEIPA(Diethonol-isopropanolamine), best raw material for cement grinding aids and concrete admixtures, performs greatly on: 

Enhancing Cement Compressive Strength At All Ages
Diethanol Isopropanolamine in cement grinding additive,,Diethanolisopropanolamine (DEIPA) is an alkanol amine used in the formulation of cement additives and concrete admixtures. 
Besides being a good grinding aid in the cement mill, DEIPA increases the...

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